Reference(s) for synthesis of (Z)-(3,3-Dimethyl)-cyclohexylideneacetaldehyde [grandlure III]
Babler, J.H., and Coghlan, M.J. 1976. A facile method for the bishomologation of ketones to alpha,ß-unsaturated aldehydes: application to the synthesis of the cyclohexanoid components of the boll weevil sex attractant. Synth. Comm. 6:469. |
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Babler, J.H., and Mortell, T.R. 1972. A facile route to three of the four terpenoid components of the boll weevil sex attractant. Tetrahedron Lett. 13:669-672. |
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Bedoukian, R.H., and Wolinsky, J. 1975. A biogenetic-type synthesis of the cyclohexyl constituents of the boll weevil pheromone. J. Org. Chem. 40:2154-2156. |
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De Souza, J.P., and Gonsalves, A.M.R. 1978. Alternative route to three of the four terpenoid components of the boll weevil sex pheromone. J. Org. Chem. 43:2068-2069. |
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Ghosh, A., Banerjee, U.K., and Venkateswaran, R.V. 1986. Decarboxylation of alpha-cyanoalkylidene esters and acids. Synthesis, of cyclohexyl constituents of the pheromone of the boll weevil. J. Chem. Res. 148. |
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Gueldner, R.C., Tumlinson, J.H., Hardee, D.D., Thompson, A.C., Hedin, P.A., and Minyard, J.P. 1971. Identification and synthesis of the four compounds comprising the boll weevil sex attractant. J. Org. Chem. 36:2616-2621. |
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Harris, F.L., and Weiler, L. 1987. The stereospecific formation of an exocyclic alkene by a consecutive radical cyclizationelimination. Tetrahedron Lett. 28:2941-2944. |
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Mandai, T., Mizobuchi, K., Kawada, M., and Otera, J. 1984. New synthetic methods for gamma-geraniol, boll weevil pheromone, and alpha-damascone employing 2-(hydroxymethyl)-4-(phenylthio)-1-butene as a building block. J. Org. Chem. 49:3403-3406. |
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Pelletier, S.W., and Mody, N.V. 1976. A facile synthesis of the cyclohexyl constituents of the boll weevil sex pheromone. J. Org. Chem. 41:1069-1071. |
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Piva, O., and Comesse, S. 2000. Tandem Michael-Wittig-Horner reaction: one-pot synthesis of delta-substituted alpha, beta-unsaturated carboxylic acid derivatives - application to a concise synthesis of (Z)- and (E)-ochtoden-1-al. Eur. J. Org. Chem. 13:2417-2424. |
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Tanaka, K., Tanikaga, R., and Kaji, A. 1976. New reagents for the synthesis of alpha,ß-unsaturated esters: lithiated O-alkyl-S-ethoxycarbonylmethyl dithiocarbonate and thiocarbonate. Chem. Lett. 917. |
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Traas, P. C., Boelens, H., and Takken, H.J. 1976. Convenient synthesis of 3,3-dimelhylcyclohexylidene acetaldehyde, a sex attractant of the male boll weevil. Synth. Comm. 6:489. |
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Tumlinson, J.H., Hardee, D.D., Gueldner, R.C., Thompson, A.C., Hedin, P.A., and Minyard, J.P. 1969. Sex pheromones produced by male boll weevil: isolation, identification, and synthesis. Science. 166:1010. |
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Vig, O.P., Ram, B., and Kaur, J. 1972. Terpenoids. Part LXXV. A new synthesis of 3,3-dimethyl-delta1,ß-cyclohexane acetaldehyde. J. Ind.Chem.Soc. 49:1181. |
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Vig, O.P., Sharma, S.D., Bari, S.S., and Kumar, S.D. 1977. Terpenoids. CXXVIII. Synthesis of 7-methyl-3-methylene-6-octen-1-ol (gamma-geraniol). Ind. J. Chem. B. 15:93. |
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Wollenberg, R.H., and Peries, R. 1979. Efficient syntheses of insect sex pheromones emitted by the boll weevil and the red bollworm moth. Tetrahedron Lett. 20:297-300. |
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